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Determination of diltiazem and its metabolites in plasma by HPLC
Summary
Type:
HPLC
Application #:
104880
Catalog#:
720949.46 - MN HPLC Column, Nucleosil C18, 100A, 3um, 4.6x150mm
Detection:
UV, 237nm
Conditions:
eluent: acetonitrile - 0.1mol/l ammonium dihydrogen phosphate buffer (37:63, v/v), containing 0.06% triethylamine, pH adjusted to 5.9 with o-phosphoric acid
flow rate 1ml/min
Authors:
Boulieu R
Source:
J Liquid Chromatogr 13 (1990) 291 - 301
Details
Legend: Fig. 2. Chromatographic separation of diltiazem and its metabolites, 1. N-demethyldeacetyldiltiazem (M2), 2. deacetyldiltiazem (M1), 3. N-demethyldiltiazem (MA), 4. diltiazem, 5. propionyl-deacetyl
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